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ASTM E2866-12(2016)

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ASTM E2866-12(2016)

Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Soil by Pressurized Fluid Extraction and Analyzed by Liquid Chromatography/Tandem Mass Spectrometry

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1.1 This procedure covers the determination of Diisopropyl Methylphosphonate (DIMP), Ethyl Methylphosphonic Acid (EMPA), Isopropyl Methylphosphonic Acid (IMPA), Methylphosphonic Acid (MPA) and Pinacolyl Methylphosphonic Acid (PMPA), referred to collectively as organophosphonates (OPs) in this test method, in soil. This method is based upon solvent extraction of a soil by pressurized fluid extraction (PFE). The extract is filtered and analyzed by liquid chromatography/tandem mass spectrometry (LC/MS/MS). OPs are qualitatively and quantitatively determined by this method.

Author ASTM
Editor ASTM
Document type Standard
Format File
Confirmation date 2016-06-01
ICS 13.080.10 : Chemical characteristics of soils
Number of pages 15
Replace ASTM E2866-12
Set ASTMVOL1104
Year 2012
Document history ASTM E2866-12
Country USA
Keyword ASTM 2866;ASTM E2866;ASTM E2866;10.1520/E2866-12R16